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Curriculum Map

Course: Separations: Distillation/Absorption

Description
This curriculum map provides a mapping of content from Perry's Chemical Engineers' Handbook to standard Separations: Distillation/Absorption course topics. The authors carefully selected relevant examples, videos, tables and figures which they felt would be valuable supplements to any standard Separations textbook. You can easily incorporate the content into your course by using our copy link functionality to paste a direct link into your school's LMS.

Authors
Don W. Green, Editor-in-Chief, Perry's Chemical Engineers' Handbook and Emeritus Distinguished Professor of Chemical and Petroleum Engineering, University of Kansas
Marylee Southard, Associate Professor, Chemical Engineering, University of Kansas

Course Topics

  • Design of Gas Absorption Systems
  • Design of Distillation Systems
  • Equipment for Distillation and Absorption

Design of Gas Absorption Systems

Relevant Material Type Description Source

Design of Gas Absorption Systems
Text
Perry's Chemical Engineers' Handbook
Introduction Text   Definitions, nomenclature, equil. data Perry's Chemical Engineers' Handbook
Nomenclature and units Table   Perry's Chemical Engineers' Handbook
Design of Gas Absorption Systems Text Design procedures Perry's Chemical Engineers' Handbook
Selection and Nature of Solvents Text Characteristics of solvents Perry's Chemical Engineers' Handbook
Gas Solubility Example Example 1, Section 14, hydrogen solubility Perry's Chemical Engineers' Handbook
Packed Tower Design Text Design equations Perry's Chemical Engineers' Handbook
Packed Height Requirement Video Example 2, Section 14 with video Perry's Chemical Engineers' Handbook
No.-Gas-Phase Mass-Trans Units Figure Figure 14-7 Perry's Chemical Engineers' Handbook
Air stripping of VOC's Video Example 3, Section 14 with video Perry's Chemical Engineers' Handbook
Tray Tower Design Text Design equations Perry's Chemical Engineers' Handbook
Actual Trays for Steam Stripping Video Example 4, Section 14 with video
Perry's Chemical Engineers' Handbook
Tray Efficiencies Figure Figure 14-9, O'Connell overall tray efficiencies Perry's Chemical Engineers' Handbook
Heat Effects in Gas Absorption Text Adiabatic and isothermal design methods Perry's Chemical Engineers' Handbook
Different Design Methods Video Example 5, Section 14 with video Perry's Chemical Engineers' Handbook
Adiabatic Method of Design Example Example 6, Section 14 Perry's Chemical Engineers' Handbook
Multicomponent Systems Text Design-absorption with no chemical reaction Perry's Chemical Engineers' Handbook
Multicomponent Absorption: Dilute System Example Example 7, Section 14 Perry's Chemical Engineers' Handbook
Multicomponent Absorption: Concentrated System Example Example 8, Section 14 Perry's Chemical Engineers' Handbook
Absorption with Chemical Reaction Text Design-absorption w/ chemical reaction Perry's Chemical Engineers' Handbook
Concentration Profiles Figure Figure 14-12; typical profiles w/ chemical reactions Perry's Chemical Engineers' Handbook
Effects of Reaction on KL Figure Figure 14-13; irreversible chemical reactions Perry's Chemical Engineers' Handbook
Effects of Packing on KGa Table Table 14-2; packing type, size and liq rate Perry's Chemical Engineers' Handbook
Typical KGa values Table Table 14-3; example systems Perry's Chemical Engineers' Handbook

Design of Distillation Systems

Relevant Material Type Description Source
Introduction Text
Perry's Chemical Engineers' Handbook
Nomenclature and Units Table
Perry's Chemical Engineers' Handbook
Thermodynamic Data and Models Text K value graphical & analytical correlations Perry's Chemical Engineers' Handbook
Vapor-liquid Equilibrium Data Text Table 13-1; selected systems Perry's Chemical Engineers' Handbook
K Values Light Hydrocarbons Figure Figure 13-9; nomograph
Perry's Chemical Engineers' Handbook
Binary Interaction Parameters Table Table 13-2; selected systems Perry's Chemical Engineers' Handbook
Antoine Vapor-Pressure Constants Table Table 13-4; selected systems; liq molar volumes
Perry's Chemical Engineers' Handbook
Graphical Methods for Binary Distillation Text Phase equil. diagrams & McCabe-Thiele Perry's Chemical Engineers' Handbook
Intermediate Reboilers/Condensers Text Includes x-y diagram Perry's Chemical Engineers' Handbook
Equation-Based Design Methods Text References to equation-based methods Perry's Chemical Engineers' Handbook
Approximate Multicomponent Methods Text FUG shortcut method; Kremser equation Perry's Chemical Engineers' Handbook
Application of FUG Method Example Example 1, Section 13; butane-pentane splitter
Perry's Chemical Engineers' Handbook
Kremser Method
Video Example 2, Section 13 with video; multicomp. absorption Perry's Chemical Engineers' Handbook
Absorption & Stripping Factors Figure Figure 13-34 Perry's Chemical Engineers' Handbook
Simulation of Distillation Processes Text Formulation of models; degrees of freedom Perry's Chemical Engineers' Handbook
Simulation Simple Distillation Column Video Example 3, Section 13 with video; butane-pentane splitter
Perry's Chemical Engineers' Handbook
Light Hydrocarbon Distillation Video Example 4, Section 13 with video; improvement of separation
Perry's Chemical Engineers' Handbook
Absorber Video Example 5, Section 13 with video; second absorber oil feed
Perry's Chemical Engineers' Handbook
Reboiled Stripper
Example
Example 6, Section 13
Perry's Chemical Engineers' Handbook
An i-Butane/n-Butane Fractionator Example
Example 7, Section13; industrial fractionator
Perry's Chemical Engineers' Handbook
Efficiency of Fractionator Video Example 8, Section 13 with video; ref. to Example 7
Perry's Chemical Engineers' Handbook
HETP of Packed Absorber
Video
Example 9, Section 13 with video; gas-plant absorber
Perry's Chemical Engineers' Handbook
Multiple Steady State in Distillation Example
Example 10, Section 13; ethanol, water, benzene
Perry's Chemical Engineers' Handbook
Mass Transfer Coefficient (Tray Column) Video Example 11, Section 13 with video
Perry's Chemical Engineers' Handbook
Mass Transfer Coefficient (Packed Column) Video Example 12, Section 13 with video
Perry's Chemical Engineers' Handbook
Nonequilibrium Model Example
Example 13, Section 13; C4 splitter
Perry's Chemical Engineers' Handbook
Need for Rigorous Models Example
Example 14, Section 13; Maxwell-Stefan model 
Perry's Chemical Engineers' Handbook
Degrees of Freedom & Design Variables Text Summary, degrees of freedom analysis
Perry's Chemical Engineers' Handbook
Distillation Systems & Configurations Text Figures showing possible configurations
Perry's Chemical Engineers' Handbook
Batch Distillation Text
Perry's Chemical Engineers' Handbook
Simple Batch Distillation Text
Basic design equations
Perry's Chemical Engineers' Handbook
Batch Distillation with Rectification Text
Solution of a simple example
Perry's Chemical Engineers' Handbook
Batch Distillation of Azeotropic Mixtures Text
Conc. paths for methanol, methyl propionate, water
Perry's Chemical Engineers' Handbook

Equipment for Distillation and Absorption

Relevant Material Type Description Source
Comparing Tray and Packed Columns Text Guidelines for column-type selection Perry's Chemical Engineers' Handbook
Factors Favoring Packing Text
Perry's Chemical Engineers' Handbook
Factors Favoring Trays Text
Perry's Chemical Engineers' Handbook
Tray Columns Text Tray, types, performance Perry's Chemical Engineers' Handbook
Flow Regimes on Trays
Text   Perry's Chemical Engineers' Handbook
Primary Tray Considerations Text Spacing, weirs, downcomers, etc. Perry's Chemical Engineers' Handbook
Other Tray Types Text Non-standard tray types Perry's Chemical Engineers' Handbook
Flooding Text Estimating flooding conditions Perry's Chemical Engineers' Handbook
Flooding of Distillation Tray Example Example 9, Section 14; sieve tray column Perry's Chemical Engineers' Handbook
Flooding Correlation Figure Figure 14-31; Fair correlation Perry's Chemical Engineers' Handbook
Maximum Downcomer Velocities Table Table 14-7 Perry's Chemical Engineers' Handbook
Derating "System" Factors Table Table 14-9; factors applied to correlations Perry's Chemical Engineers' Handbook
Entrainment Text Effects of fluid rates & other variables Perry's Chemical Engineers' Handbook
Entrainment Effect on Tray Efficiency Example Example 10, Section 14; ref to Example 9 Perry's Chemical Engineers' Handbook
Entrainment Correlation Figure Figure 14-34; entrainment as function of L/G Perry's Chemical Engineers' Handbook
Pressure Drop Text Calculation of pressure drop through column
Perry's Chemical Engineers' Handbook
Pressure Drop, Sieve Tray Example Example 11, Section 14; ref to Example 9
Perry's Chemical Engineers' Handbook
Other Hydraulic Limits Text Weeping, dumping, vapor channeling
Perry's Chemical Engineers' Handbook
Tray Efficiency Text Definitions & estimation of tray efficiencies
Perry's Chemical Engineers' Handbook
Representative Tray Efficiencies Table Table 14-12; sieve & valve trays
Perry's Chemical Engineers' Handbook
Estimating Tray Efficiency Example Example 12, Section 14; ref to Example 9
Perry's Chemical Engineers' Handbook
Packed Columns Text
Perry's Chemical Engineers' Handbook
Packing Objectives Text Major objectives in selecting packed column 
Perry's Chemical Engineers' Handbook
Packed-Column Flood & Pressure Drop Text Guidelines for operating conditions
Perry's Chemical Engineers' Handbook
Generalized Pressure Drop Correlation Figure Figure 14-55; Eckert correlation; GPDC
Perry's Chemical Engineers' Handbook
Pressure Drop Correlation Figure Figure 14-56; Kister & Gill GPDC
Perry's Chemical Engineers' Handbook
Characteristics of Random Packings Table Table 14-13; characteristics of numerous packings
Perry's Chemical Engineers' Handbook
Characteristics of Structured Packings Table Table 14-14; characteristics of numerous packings
Perry's Chemical Engineers' Handbook
Packed Column Pressure Drop Example Example 13, Section14; bed of 2 in Pall Rings
Perry's Chemical Engineers' Handbook
Packing Efficiency Text HETP discussion, effects of poor distribution
Perry's Chemical Engineers' Handbook
Packed-Tower Scale-Up Text Scale-up disc of several parameters
Perry's Chemical Engineers' Handbook
Gas & Liquid Equipment Text Additional topics, comparison packed vs. tray
Perry's Chemical Engineers' Handbook
Wetted Wall Columns Text Mass transfer effects discussed
Perry's Chemical Engineers' Handbook
Liquid Film Resistance Figure Figure 14-79; absorption of gases
Perry's Chemical Engineers' Handbook
Column Costs Text Cost tables & figures
Perry's Chemical Engineers' Handbook

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